Dans un ballon à col rôdé, introdui

Dans un ballon à col rôdé, introduire une prise d’essai p, exactement pesée voisine de 2,8 g de produit, 5 mL d’isopropanol et agiter au vortex.
Ajouter 20 mL de réactif 1, agiter dans un bain à ultra-sons puis chauffer à ébullition sous reflux pendant 5 min
Après refroidissement, transvaser dans une fiole jaugée de 100 mL en lavant le ballon avec de l’eau distillée. Compléter au volume avec les eaux de lavage.
Filtrer sur Stérivex 0.22 µm ou équivalent.
Filtrer 1ère fois sur filtre embout seringue composé d’une membrane en polypropylène de porosité 0,45 µm. (Equivalent acrodisc GHP). Puis une 2ème fois sur le même type de filtre de porosité 0,2 µm.

결과 (영어) 1:

In a balloon to oiled neck, introduce a test socket p, exactly next weighing 2.8 g of product, 5 mL of isopropanol and vortex.Add 20 mL of reagent 1, shake in a ultrasonic bath, then heat to boiling under reflux for 5 minAfter cooling, transfer to a measured 100 ml vial washing ball with distilled water. Make up to the volume with the wash water.Filter on Sterivex 0.22 µm or equivalent.Filter 1st time on filter tip syringe composed of a polypropylene porosity 0.45 µm. (Equivalent acrodisc GHP) membrane. Then a 2nd time on the same type of porosity filter 0.2 µm.

결과 (영어) 2:

In a balloon prowled collar, introduce a per test sample, accurately weighed 2.8 g of product, 5 mL of isopropanol and vortex.
Add 20 ml of reagent 1, mix in a hot ultra- sounds and heat to boiling under reflux for 5 min
After cooling, transfer to a volumetric flask of 100 mL by washing it with distilled water. Make up to volume with the washing water.
Filter through Sterivex 0.22 .mu.m or equivalent.
Filter 1st time on syringe tip filter consisting of a polypropylene membrane of porosity 0.45 .mu.m. (Equivalent acrodisc GHP). Then a second time on the same type of filter porosity of 0.2 microns.

결과 (영어) 3:

in a ball to pass run, place a sample p, accurately weighed close to 2.8 g of the product, 5 ml of isopropanol and a vortex.add 20 ml of reagent, stirring in a bath with ultrasonic and heat to boiling under reflux for 5 minutes.after cooling, transfer to a 100 ml volumetric flask by washing it with distilled water, make up to volume with the wash water.on stérivex 0.22 m filter or equivalent.first tip syringe filter filter consisting of a porous polypropylene membrane of 0.45 mm (equivalent acrodisc region). then a second time on the same type of filter porosity 0.2 microns.